1-(2-Methoxyphenyl)piperazine → HCID 13729392, compound

HRID 1906440Notes

Reaction equation

HRID 1906440 reaction equation
[C:1]([C:4]1[O:5][C:6]2[CH:12]=[C:11]([O:13][CH2:14][CH:15]3[O:17][CH2:16]3)[CH:10]=[CH:9][C:7]=2[CH:8]=1)(=[O:3])[NH2:2].[CH3:18][O:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][C:21]=1[N:26]1[CH2:31][CH2:30][NH:29][CH2:28][CH2:27]1>>[C:1]([C:4]1[O:5][C:6]2[CH:12]=[C:11]([O:13][CH2:14][CH:15]([OH:17])[CH2:16][N:29]3[CH2:28][CH2:27][N:26]([C:21]4[CH:22]=[CH:23][CH:24]=[CH:25][C:20]=4[O:19][CH3:18])[CH2:31][CH2:30]3)[CH:10]=[CH:9][C:7]=2[CH:8]=1)(=[O:3])[NH2:2]

Participants

3

Reactant 2

HCID 13461-(2-Methoxyphenyl)piperazineHCID 13729404HCID 13729404, compound

Product 1

HCID 13729392HCID 13729392, compound

Procedure

The procedures of Example 8a were repeated except that 1.2 g (0.005 mole) of 2-carbamoyl-6-(2,3-epoxypropoxy)benzofuran and 1.1 g (0.0055 mole) of 1-(2-methoxyphenyl)piperazine were employed to give the desired compound.

Sources & evidence

ORD record
ord-5af491faaa874304b2c47f0e049e6b83
Source dataset
uspto-grants-1987_03
Patent number
US04652566

Reaction notes

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