HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl alpha-acetamidocinnamate → Acetylphenylalanine methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl alpha-acetamidocinnamate | HCID 340163 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Acetylphenylalanine methyl ester | HCID 704002 | 82.4% |
Reaction Steps
A second recycling of the catalyst is performed under the conditions described above, but introducing methyl α-acetamidocinnamate (1.6 g) and ethyl acetate (10 cc). Pure N-acetylphenylalanine methyl ester (1.33 g) is thus obtained with a conversion of 100%, its rotatory power being:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04654176 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-e343201433b347ff99acb0176de1801c |
| Source note | uspto-grants-1987_03 |