HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzyl mercaptan → Emd 39593
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzyl mercaptan | HCID 580759 | — |
| Reactant | 4-chloro-1-methyl-1H-imidazo(4,5-c)pyridine | HCID 948792 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Emd 39593 | HCID 135146 | — |
Reaction Steps
2.76 g of Na is dissolved in 180 ml of ethanol; 19.1 g of o-chlorobenzylmercaptan and 16.76 g of 4-chloro-1-methyl-1H-imidazo(4,5-c)pyridine are added; the mixture is boiled for 16 hours and evaporated; and the residue is worked up in the customary manner to give 4-o-chloro-benzylthio-1-methyl-1H-imidazo(4,5-c)pyridine of m.p. 152°-155° (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04654350 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-356079d3f1214307a783e51e9d01b193 |
| Source note | uspto-grants-1987_03 |