Phenyl isocyanate → HCID 20210821, compound

HRID 1906745Notes

Reaction equation

HRID 1906745 reaction equation
Cl.[OH:2][CH2:3][CH:4]([CH2:26][OH:27])[CH:5]1[C:14]2[C:9](=[CH:10][C:11]([O:17][CH3:18])=[C:12]([O:15][CH3:16])[CH:13]=2)[CH2:8][CH2:7][N:6]1[CH2:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1.[C:28]1([N:34]=[C:35]=[O:36])[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1>>[C:28]1([NH:34][C:35]([O:2][CH2:3][CH:4]([CH2:26][O:27][C:35](=[O:36])[NH:34][C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[CH:5]2[C:14]3[C:9](=[CH:10][C:11]([O:17][CH3:18])=[C:12]([O:15][CH3:16])[CH:13]=3)[CH2:8][CH2:7][N:6]2[CH2:19][C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=2)=[O:36])[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1

Participants

3

Reactant 2

HCID 7672Phenyl isocyanateHCID 20200547HCID 20200547, compound

Product 1

HCID 20210821HCID 20210821, compound

Procedure

0.01 mole of the compound obtained in Step (A) is boiled with 0.02 mole of phenyl isocyanate for 4 to 6 hours. Evaporation of the reaction mixture yields the aimed compound in a crystalline form.

Workup

  1. customEvaporation of the reaction mixture

Sources & evidence

ORD record
ord-4b10cad607da41049a0a385fc7764728
Source dataset
uspto-grants-1987_03
Patent number
US04654351

Reaction notes

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