1-Bromododecane → HCID 20210667, compound

HRID 1906765Notes

Reaction equation

HRID 1906765 reaction equation
[C:1]1([N:7]2[C:24]([OH:25])=[C:10]3[N:11]=[CH:12][N:13]=[C:14]([S:15][C:16]([C:19]([O:21][CH2:22][CH3:23])=[O:20])([CH3:18])[CH3:17])[C:9]3=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:26](Br)[CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37]>>[C:1]1([N:7]2[C:24]([O:25][CH2:37][CH2:36][CH2:35][CH2:34][CH2:33][CH2:32][CH2:31][CH2:30][CH2:29][CH2:28][CH2:27][CH3:26])=[C:10]3[N:11]=[CH:12][N:13]=[C:14]([S:15][C:16]([C:19]([O:21][CH2:22][CH3:23])=[O:20])([CH3:18])[CH3:17])[C:9]3=[N:8]2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 89191-BromododecaneHCID 178471745HCID 178471745, compound

Product 1

HCID 20210667HCID 20210667, compoundYield 30%

Procedure

1 g of 2-phenyl-3-hydroxy-7-(1-ethoxycarbonyl-1-methyl-ethylthio)-pyrazolo[4,3-d]pyrimidine and 0.84 g of n-dodecyl bromide were reacted and treated in the same manner as in Example 31 to obtain the desired product.

Workup

  1. additiontreated in the same manner as in Example 31

Sources & evidence

ORD record
ord-335a2c6f69d846eab8c365ff96af4f25
Source dataset
uspto-grants-1987_03
Patent number
US04654348

Reaction notes

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