Sodium Hydroxide → HCID 70434660, compound

HRID 1906834Notes

Reaction equation

HRID 1906834 reaction equation
[C:1]1([N:7]2[C:11]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)=[C:10]([C:18]3[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=3)[N:9]=[C:8]2[S:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][C:32]([OH:34])=[O:33])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH-].[Na+:36]>C(O)C>[Na+:36].[C:1]1([N:7]2[C:11]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)=[C:10]([C:18]3[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=3)[N:9]=[C:8]2[S:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][C:32]([O-:34])=[O:33])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 13453787HCID 13453787, compound

Product 1

HCID 70434660HCID 70434660, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent2×

Procedure

12 g of 8-(1.4.5-triphenylimidazol-2-yl mercapto)-octanoic acid are dissolved in 250 cc. of 96% ethanol. The equivalent amount of ethanolic sodalye (1 g of NaOH in 10 cc. of ethanol) is added and the mixture is stirred for a short time and evaporated to dryness in a vacuo. The residue is pulverized.

Workup

  1. customevaporated to dryness in a vacuo

Sources & evidence

ORD record
ord-8d696b27f5aa4966ad97580e08d48fb3
Source dataset
uspto-grants-1987_03
Patent number
US04654358

Reaction notes

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