HuagongsheHuagongshe Chemistry Print Report · For research reference only
3'-Aminoacetophenone → HCID 673709, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3'-Aminoacetophenone | HCID 7417 | — |
| Reactant | Cyclopropanecarbonyl chloride | HCID 77637 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 673709 | HCID 673709 | — |
Reaction Steps
A mixture of 13.524 g of m-aminoacetophenone and 14.224 g of diisopropylethylamine in 300 ml of dichloromethane was stirred with cooling. An 11.45 g portion of cyclopropanecarboxylic acid chloride was added and the mixture was stirred at room temperature overnight. The solid was collected, giving 17.30 g of N-(3-acetylphenyl)cyclopropanecarboxamide, mp 136°-137° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04654347 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-84b409c28ef54f908e6877bec5fdfc4a |
| Source note | uspto-grants-1987_03 |