Methyl iodide → HCID 86741389, compound

HRID 1906843Notes

Reaction equation

[CH3:1][N:2]([CH3:18])[CH:3]=[CH:4][C:5]([C:7]1[CH:8]=[C:9]([NH:13][C:14](=[O:17])[O:15][CH3:16])[CH:10]=[CH:11][CH:12]=1)=[O:6].[CH3:19]I>>[CH3:18][N:2]([CH3:1])[CH:3]=[CH:4][C:5]([C:7]1[CH:8]=[C:9]([N:13]([CH3:19])[C:14](=[O:17])[O:15][CH3:16])[CH:10]=[CH:11][CH:12]=1)=[O:6]

Participants

Reactant 2

HCID 6328Methyl iodide

HCID 53959556HCID 53959556, compound

Product 1

HCID 86741389HCID 86741389, compound

Procedure

A 9.93 g portion of [3-[3-(dimethylamino)-1-oxo-2-propenyl]phenyl]carbamic acid, methyl ester was alkylated as described in Example 3, using 6.82 g of methyl iodide, giving 10.13 g of the desired compound, mp 93°-95° C.

Sources & evidence

ORD record: ord-1c98459f1ab74bb99af920347a4c65b8
Source dataset: uspto-grants-1987_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04654347

Reaction notes

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