HuagongsheHuagongshe Chemistry Print Report · For research reference only
3'-Aminoacetophenone → ethyl N-(3-acetylphenyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3'-Aminoacetophenone | HCID 7417 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | ethyl N-(3-acetylphenyl)carbamate | HCID 717681 | 91.5% |
Reaction Steps
A mixture of 27.03 g of m-aminoacetophenone, 27.14 g of diisopropylethylamine, 22.8 g of ethylchloroformate and 300 ml of dichloromethane was reacted as described in Example 1, giving 37.9 g of (3-acetylphenyl)carbamic acid, ethyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04654347 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-0da99adbf7914f9daf2cbe3634a78a95 |
| Source note | uspto-grants-1987_03 |