HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 178492057, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 178492058 | HCID 178492058 | — |
| Reactant | HCID 178515209 | HCID 178515209 | — |
| Product | HCID 178492057 | HCID 178492057 | — |
Reaction Steps
The title compound was prepared following the procedure for 7a using 6c and 1-methylpiperazine. 1H-NMR (DMSO-d6) δ (ppm): 3.25 (4H, br), 3.45 (3H, s), 3.50 (4H, br), 3.75 (3H, s), 7.00 (1H, d, J=9.06 Hz), 7.40 (1H, m), 7.48 (1H, br), 7.68 (1H, d, J=9.06 Hz), 7.92 (1H, d, J=8.79 Hz), 8.05 (2H, d, J=8.79 Hz), 8.56 (1H, br), 9.12 (1H, br). m/z 390.4 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598159B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-25b2593a3cef4cc4a41ba68ad5af71df |
| Source note | uspto-grants-2013_12 |