HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3,5-Dimethoxyphenyl)piperazine → Supinoxin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3,5-Dimethoxyphenyl)piperazine | HCID 2736205 | — |
| Reactant | Ethyl N-(6-fluoro-2-methoxyquinoxalin-3-yl)carbamate | HCID 66917965 | — |
| Product | Supinoxin | HCID 11619093 | 72% |
Reaction Steps
Ethyl N-(6-fluoro-2-methoxyquinoxalin-3-yl)carbamate and 1-(3,5-dimethoxyphenyl)piperazine were reacted by the same way with the example 1 to obtain the titled compound (yield, 72%). MS(ESI) m/z 442 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-7d652cdf8f724b30a223ca6d4de62db0 |
| Source note | uspto-grants-2013_12 |