HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3,4,5-Trimethoxyphenyl)piperazine → HCID 66917977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3,4,5-Trimethoxyphenyl)piperazine | HCID 3838765 | — |
| Reactant | Ethyl N-(6-chloro-2-methoxyquinoxalin-3-yl)carbamate | HCID 66918182 | — |
| Product | HCID 66917977 | HCID 66917977 | 84% |
Reaction Steps
Ethyl N-(6-chloro-2-methoxyquinoxalin-3-yl)carbamate and 1-(3,4,5-trimethoxyphenyl)piperazine were reacted by the same way with the example 22 to obtain the titled compound (yield, 84%). 1H NMR (300 MHz, CDCl3): δ 3.17-3.25 (m, 4H), 3.81-3.86 (m, 12H), 4.09-4.16 (m, 4H), 6.21 (s, 2H), 7.21-7.30 (m, 1H), 7.33-7.54 (m, 1H), 7.58-7.69 (m, 1H), 7.81 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-32e98b96c625443c987654a00b052fbe |
| Source note | uspto-grants-2013_12 |