HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2,6-Xylyl)piperazine → HCID 66918084, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2,6-Xylyl)piperazine | HCID 70538 | — |
| Reactant | Ethyl N-(2,6-dimethoxyquinoxalin-3-yl)carbamate | HCID 66918080 | — |
| Product | HCID 66918084 | HCID 66918084 | 87% |
Reaction Steps
Ethyl N-(2,6-dimethoxyquinoxalin-3-yl)carbamate and 1-(2,6-dimethylphenyl)piperazine were reacted by the same way with the example 64 to obtain the titled compound (yield, 87%). 1H NMR (300 MHz, CDCl3): δ 2.33-2.36 (m, 6H), 3.14-3.22 (m, 4H), 3.70-3.90 (m, 6H), 4.09-4.15 (m, 4H), 6.67-7.32 (m, 6H), 7.50-7.65 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-d8c320be8d9d46c5aa96d86016ae29fd |
| Source note | uspto-grants-2013_12 |