HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Fluorophenyl)piperazine → HCID 69243276, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Fluorophenyl)piperazine | HCID 75260 | — |
| Reactant | ethyl N-(6-fluoro-3-methoxyquinoxalin-2-yl)carbamate | HCID 69243333 | — |
| Product | HCID 69243276 | HCID 69243276 | 82% |
Reaction Steps
Ethyl N-(6-fluoro-3-methoxyquinoxalin-2-yl)carbamate and 1-(4-fluorophenyl)piperazine were reacted by the same way with the example 85 to obtain the titled compound (yield, 82%). 1H NMR (300 MHz, CDCl3): δ 3.18-3.21 (m, 4H), 3.74-3.78 (m, 4H), 4.14 (s, 3H), 6.88-6.92 (m, 4H), 7.25-7.42 (m, 3H), 7.76-7.81 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-02324998d9634c80978f7aba06461e8e |
| Source note | uspto-grants-2013_12 |