HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3,5-Dimethylphenyl)piperazine → HCID 69245223, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3,5-Dimethylphenyl)piperazine | HCID 2758626 | — |
| Reactant | ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate | HCID 69241674 | — |
| Product | HCID 69245223 | HCID 69245223 | 85% |
Reaction Steps
Ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate and 1-(3,5-dimethylphenyl)piperazine were reacted by the same way with the example 106 to obtain the titled compound (yield, 85%). 1H NMR (300 MHz, CDCl3): δ 2.29 (s, 6H), 3.25-3.29 (m, 4H), 3.73-3.76 (m, 4H), 4.15 (s, 3H), 6.59 (s, 3H), 7.30-7.49 (m, 3H), 7.74-7.77 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-6d1133e1f2f9405b95d8ad1b0eb528ec |
| Source note | uspto-grants-2013_12 |