HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Chlorophenyl)piperazine → HCID 69242324, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Chlorophenyl)piperazine | HCID 1355 | — |
| Reactant | ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate | HCID 69241674 | — |
| Product | HCID 69242324 | HCID 69242324 | 86% |
Reaction Steps
Ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate and 1-(3-chlorophenyl)piperazine were reacted by the same way with the example 106 to obtain the titled compound (yield, 86%). 1H NMR (300 MHz, CDCl3): δ 3.30 (s, 4H), 3.76 (s, 4H), 4.15 (s, 3H), 6.79-6.90 (m, 3H), 7.15-7.45 (m, 3H), 7.62-7.75 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-6d1ae3d49b38422a908c1e61afdc5289 |
| Source note | uspto-grants-2013_12 |