HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Chlorophenyl)piperazine → HCID 69242558, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Chlorophenyl)piperazine | HCID 97478 | — |
| Reactant | ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate | HCID 69241674 | — |
| Product | HCID 69242558 | HCID 69242558 | 94% |
Reaction Steps
Ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate and 1-(4-chlorophenyl)piperazine were reacted by the same way with the example 106 to obtain the titled compound (yield, 94%). 1H NMR (300 MHz, CDCl3): δ 3.25 (s, 4H), 3.76 (s, 4H), 4.15 (s, 3H), 6.86 (d, J=9.0 Hz, 2H), 7.22-7.45 (m, 4H), 7.72-7.75 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-e1ca388b9a4c4806bb63dc43137f0e60 |
| Source note | uspto-grants-2013_12 |