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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1907574Generated: October 31, 2026

1-(2-Pyrimidinyl)piperazine → HCID 69242403, compound

https://huagongshe.com/reaction/1907574

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(2-Pyrimidinyl)piperazineHCID 88747—
Reactantethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamateHCID 69241674—
ProductHCID 69242403HCID 6924240390%

Reaction Steps

Ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate and 1-(2-pyrimidyl)piperazine were reacted by the same way with the example 106 to obtain the titled compound (yield, 90%). 1H NMR (300 MHz, CDCl3): δ 3.69-3.73 (m, 4H), 3.98 (s, 4H), 4.16 (s, 3H), 6.54-6.55 (m, 1H), 7.28-7.49 (m, 1H), 7.63-7.75 (m, 2H), 8.33 (d, J=4.8 Hz, 2H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08598173B2
Source datasetuspto-grants-2013_12
ORD IDord-8504b09c3f4c4beb86b198be92ca57f7
Source noteuspto-grants-2013_12