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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1907586Generated: October 31, 2026

1-(2,6-Xylyl)piperazine → HCID 69245227, compound

https://huagongshe.com/reaction/1907586

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(2,6-Xylyl)piperazineHCID 70538—
Reactantethyl N-(3-methoxy-6-methylquinoxalin-2-yl)carbamateHCID 69243736—
ProductHCID 69245227HCID 6924522783%

Reaction Steps

Ethyl N-(3-methoxy-6-methylquinoxalin-2-yl)carbamate and 1-(2,6-dimethylphenyl)piperazine were reacted by the same way with the example 127 to obtain the titled compound (yield, 83%). 1H NMR (300 MHz, CDCl3): δ 2.33-2.50 (m, 9H), 3.14-2.20 (m, 4H), 3.70-3.75 (m, 4H), 4.14 (s, 3H), 7.00 (s, 3H), 7.09-7.78 (m, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08598173B2
Source datasetuspto-grants-2013_12
ORD IDord-5291ce83b75e40378415326c99588981
Source noteuspto-grants-2013_12