HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Fluorophenyl)piperazine → HCID 69240962, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Fluorophenyl)piperazine | HCID 70529 | — |
| Reactant | ethyl N-(3-methoxy-6-methylquinoxalin-2-yl)carbamate | HCID 69243736 | — |
| Product | HCID 69240962 | HCID 69240962 | 98% |
Reaction Steps
Ethyl N-(3-methoxy-6-methylquinoxalin-2-yl)carbamate and 1-(2-fluorophenyl)piperazine were reacted by the same way with the example 127 to obtain the titled compound (yield, 98%). 1H NMR (300 MHz, CDCl3): δ 2.49 (s, 3H), 3.11-3.18 (m, 4H), 3.77-3.86 (m, 4H), 4.12 (s, 3H), 6.95-7.61 (m, 7H), 7.73 (d, J=8.6 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-23121ad99917486abff4fba8a3a0e4c8 |
| Source note | uspto-grants-2013_12 |