HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-Cyanophenyl)piperazine → HCID 69242464, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-Cyanophenyl)piperazine | HCID 2735875 | — |
| Reactant | ethyl N-(3-methoxy-6-methylquinoxalin-2-yl)carbamate | HCID 69243736 | — |
| Product | HCID 69242464 | HCID 69242464 | 93% |
Reaction Steps
Ethyl N-(3-methoxy-6-methylquinoxalin-2-yl)carbamate and 1-(2-cyanophenyl)piperazine were reacted by the same way with the example 127 to obtain the titled compound (yield, 93%). 1H NMR (300 MHz, CDCl3): δ 2.47 (s, 3H), 3.20-3.28 (m, 4H), 3.76-3.96 (m, 4H), 4.14 (s, 3H), 7.02-7.13 (m, 3H), 7.28 (s, 1H), 7.49-7.63 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-f973649ede524b9b9cc1f34378369ac4 |
| Source note | uspto-grants-2013_12 |