HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Methoxyphenyl)piperazine → HCID 69242413, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Methoxyphenyl)piperazine | HCID 1346 | — |
| Reactant | ethyl N-(3,6-dimethoxyquinoxalin-2-yl)carbamate | HCID 69244324 | — |
| Product | HCID 69242413 | HCID 69242413 | 84% |
Reaction Steps
Ethyl N-(3,6-dimethoxyquinoxalin-2-yl)carbamate and 1-(2-methoxyphenyl)piperazine were reacted by the same way with the example 148 to obtain the titled compound (yield, 84%). 1H NMR (300 MHz, CDCl3): δ 3.13-3.16 (m, 4H), 3.66-3.78 (m, 4H), 3.88 (s, 3H), 3.90 (s, 3H), 4.12 (s, 3H), 6.87-7.14 (m, 7H), 7.76 (d, J=5.1 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-4ec11de32c9b48fc84bbaf43d13dcfa6 |
| Source note | uspto-grants-2013_12 |