HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Chlorophenyl)piperazine → HCID 69243066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Chlorophenyl)piperazine | HCID 415628 | — |
| Reactant | ethyl N-(3,6-dimethoxyquinoxalin-2-yl)carbamate | HCID 69244324 | — |
| Product | HCID 69243066 | HCID 69243066 | 89% |
Reaction Steps
Ethyl N-(3,6-dimethoxyquinoxalin-2-yl)carbamate and 1-(2-chlorophenyl)piperazine were reacted by the same way with the example 148 to obtain the titled compound (yield, 89%). 1H NMR (300 MHz, CDCl3): δ 3.13 (s, 4H), 3.78 (s, 4H), 3.90 (s, 3H), 4.12 (s, 3H), 6.98-7.37 (m, 7H), 7.76 (d, J=9.9 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-e547d8af5517458788bffd8aa4422a56 |
| Source note | uspto-grants-2013_12 |