HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Chlorophenyl)piperazine → HCID 69244367, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Chlorophenyl)piperazine | HCID 97478 | — |
| Reactant | ethyl N-(3,6-dimethoxyquinoxalin-2-yl)carbamate | HCID 69244324 | — |
| Product | HCID 69244367 | HCID 69244367 | 93% |
Reaction Steps
Ethyl N-(3,6-dimethoxyquinoxalin-2-yl)carbamate and 1-(4-chlorophenyl)piperazine were reacted by the same way with the example 148 to obtain the titled compound (yield, 93%). 1H NMR (300 MHz, CDCl3): δ 3.23 (s, 4H), 3.75 (s, 4H), 3.90 (s, 3H), 4.13 (s, 3H), 6.85 (d, J=9.0 Hz, 2H), 7.14 (s, 2H), 7.20-7.25 (m, 3H), 7.71-7.74 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-6a74d730e68746c09bd994777f73665c |
| Source note | uspto-grants-2013_12 |