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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1907635Generated: October 31, 2026

1-(3-Bromophenyl)piperazine → HCID 69241098, compound

https://huagongshe.com/reaction/1907635

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(3-Bromophenyl)piperazineHCID 2757154—
ReactantEthyl N-(6,7-dichloro-2-methoxyquinoxalin-3-yl)carbamateHCID 69243293—
ProductHCID 69241098HCID 6924109872%

Reaction Steps

Ethyl N-(6,7-dichloro-2-methoxyquinoxalin-3-yl)carbamate and 1-(3-bromophenyl)piperazine were reacted by the same way with the example 176 to obtain the titled compound (yield, 72%). 1H NMR (300 MHz, CDCl3) δ 3.29-3.31 (m, 4H), 3.74-3.76 (m, 4H), 4.16 (s, 3H), 6.85-6.87 (m, 1H), 7.02-7.04 (m, 1H), 7.06-7.07 (m, 1H), 7.13-7.15 (m, 1H), 7.32 (br s, 1H), 7.86 (br s, 1H), 7.86 (br s, 1H), 7.91 (br s, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08598173B2
Source datasetuspto-grants-2013_12
ORD IDord-ea8e067aad724182bb2ddfabbbabca3b
Source noteuspto-grants-2013_12