HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Bromophenyl)piperazine → HCID 69241098, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Bromophenyl)piperazine | HCID 2757154 | — |
| Reactant | Ethyl N-(6,7-dichloro-2-methoxyquinoxalin-3-yl)carbamate | HCID 69243293 | — |
| Product | HCID 69241098 | HCID 69241098 | 72% |
Reaction Steps
Ethyl N-(6,7-dichloro-2-methoxyquinoxalin-3-yl)carbamate and 1-(3-bromophenyl)piperazine were reacted by the same way with the example 176 to obtain the titled compound (yield, 72%). 1H NMR (300 MHz, CDCl3) δ 3.29-3.31 (m, 4H), 3.74-3.76 (m, 4H), 4.16 (s, 3H), 6.85-6.87 (m, 1H), 7.02-7.04 (m, 1H), 7.06-7.07 (m, 1H), 7.13-7.15 (m, 1H), 7.32 (br s, 1H), 7.86 (br s, 1H), 7.86 (br s, 1H), 7.91 (br s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-ea8e067aad724182bb2ddfabbbabca3b |
| Source note | uspto-grants-2013_12 |