HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1907768Generated: October 31, 2026
3-(2-Bromoacetyl)pyridine → HCID 59737476, compound
https://huagongshe.com/reaction/1907768
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-(2-Bromoacetyl)pyridine | HCID 151408 | — |
| Reactant | 1-(4-Ethoxycarbonylphenyl)-2-thiourea | HCID 2808848 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 59737476 | HCID 59737476 | 166.2% |
Reaction Steps
Ethyl 4-thioureidobenzoate (209 mg, 0.935 mmol) was added to a warm solution (50° C.) of 2-bromo-1-(pyridin-3-yl)ethanone (250 mg, 0.88 mmol) in water (5 mL) and stirred at 50° C. for 5 h. The precipitated was filtered out to afford the title compound 428 as a yellow solid (476 mg, wet) which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08598168B2 |
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| Source dataset | uspto-grants-2013_12 |
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| ORD ID | ord-a7a2d34652254ee7a28861f766b5f591 |
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| Source note | uspto-grants-2013_12 |
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