Tetrabutylammonium Fluoride → HCID 59737244, compound

Participants

Reaction Steps

TBAF (26 μL) was added to a solution of 440 (14 mg, 0.027 mmol) in THF (50 μL), stirred 1 h at room temperature, diluted with ethyl, washed with water, the organic layer was dried (MgSO4), filtered and concentrated. The compound was purified by preparative TLC to afford the title compound 441 (5.4 mg, 56% yield).

Provenance & Evidence