Hydrogen Peroxide → HCID 178491580, compound

Participants

Reaction Steps

A solution of compound 461 (0.55 g, 1.31 mmol) and ReO3Me (33 mg, 0.13 mmol) in DCM (10 mL) was stirred 5 min, 35% H2O2 (0.14 mL, 1.53 mmol) was added and the reaction was stirred at room temperature for 2 h. The reaction mixture was quenched with water, and AcOEt was added. The white precipitate was filtered and washed with AcOEt and MeOH (5 mL) to afford the title compound 462 (350 mg, 61%) as a white solid.

Provenance & Evidence