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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1907865Generated: November 4, 2026

Hydrogen Bromide → HCID 68577348, compound

https://huagongshe.com/reaction/1907865

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrogen BromideHCID 260—
ReactantHCID 25117356HCID 25117356—
SolventAcetic AcidHCID 176—
ProductHCID 68577348HCID 6857734897.5%

Reaction Steps

0.085 g (0.23 mmol) of [2-(1-methyl-6-oxo-1,6-dihydro-[4,4′]bipyrimidinyl-2-yl)-ethyl]-carbamic acid benzyl ester was dissolved in 0.164 g (1.16 mmol) of hydrobromide acid in acetic acid. The resulting mixture was stirred at room temperature for 2 h. The resulting precipitate was filtered, washed with diethyl ether and dried to afford 0.07 g of a yellow compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08598187B2
Source datasetuspto-grants-2013_12
ORD IDord-ce78b3f87a22474cb93638a2ce474217
Source noteuspto-grants-2013_12