HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 68577348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 25117356 | HCID 25117356 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 68577348 | HCID 68577348 | 97.5% |
Reaction Steps
0.085 g (0.23 mmol) of [2-(1-methyl-6-oxo-1,6-dihydro-[4,4′]bipyrimidinyl-2-yl)-ethyl]-carbamic acid benzyl ester was dissolved in 0.164 g (1.16 mmol) of hydrobromide acid in acetic acid. The resulting mixture was stirred at room temperature for 2 h. The resulting precipitate was filtered, washed with diethyl ether and dried to afford 0.07 g of a yellow compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598187B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-ce78b3f87a22474cb93638a2ce474217 |
| Source note | uspto-grants-2013_12 |