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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1908708Generated: October 29, 2026

Heptane → HCID 46830963, compound

https://huagongshe.com/reaction/1908708

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHeptaneHCID 8900—
ReactantHCID 46830960HCID 46830960—
SolventEthyl AcetateHCID 8857—
ProductHCID 46830963HCID 4683096380.2%

Reaction Conditions

Temperature0 °C

Reaction Steps

The compound (50 mg) prepared in Example 10 (2) was dissolved in ethyl acetate (1.4 mL) at 70° C. To the solution, n-heptane (0.68 mL) was added at room temperature, which was then cooled to 0° C. The crystal was filtered and dried under reduced pressure to obtain the title compound (39 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08598223B2
Source datasetuspto-grants-2013_12
ORD IDord-ff80d9ce76b64020b5aa9a59a2679f0d
Source noteuspto-grants-2013_12