Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Heptane | HCID 8900 | — |
| Reactant | HCID 46830960 | HCID 46830960 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 46830963 | HCID 46830963 | 80.2% |
Reaction Steps
The compound (50 mg) prepared in Example 10 (2) was dissolved in ethyl acetate (1.4 mL) at 70° C. To the solution, n-heptane (0.68 mL) was added at room temperature, which was then cooled to 0° C. The crystal was filtered and dried under reduced pressure to obtain the title compound (39 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08598223B2 |
|---|
| Source dataset | uspto-grants-2013_12 |
|---|
| ORD ID | ord-ff80d9ce76b64020b5aa9a59a2679f0d |
|---|
| Source note | uspto-grants-2013_12 |
|---|