HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylisopropylamine → 2-(Isopropyl-methyl-amino)-6-methyl-isonicotinic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylisopropylamine | HCID 78485 | — |
| Reactant | 2-(Diethylamino)-6-methylisonicotinic acid hydrochloride | HCID 67026972 | — |
| Product | 2-(Isopropyl-methyl-amino)-6-methyl-isonicotinic acid | HCID 58418004 | — |
Reaction Steps
The title compound is prepared in analogy to 2-diethylamino-6-methyl-isonicotinic acid hydrochloride using isopropylmethylamine; LC-MS: tR=0.54 min; [M+H]+=209.09; 1H NMR δ 1.37 (d, J=6.3 Hz, 6H), 2.64 (s, 3H), 3.17 (s, 3H), 4.50-4.60 (m, 1H), 7.16 (s, 1H), 7.62 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598208B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-4e3582de711f43ed85392bb42a5ba029 |
| Source note | uspto-grants-2013_12 |