HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(2-Dimethylamino-ethoxy)-2-nitro-phenylamine → 4-(2-(Dimethylamino)ethoxy)benzene-1,2-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(2-Dimethylamino-ethoxy)-2-nitro-phenylamine | HCID 20376745 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-(2-(Dimethylamino)ethoxy)benzene-1,2-diamine | HCID 22167701 | 90.3% |
Reaction Steps
5-(2-Dimethylamino-ethoxy)-2-nitro-phenylamine (0.85 g, 3.77 mmol) was dissolved in EtOH and shaken under an atmosphere of H2 for 6 hours. The catalyst was removed by filtration. Evaporation in vacuo gave 4-(2-Dimethylamino-ethoxy)-benzene-1,2-diamine as a dark yellow oil (0.665 g, 90%). MS(ESI) m/z 196.0 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598217B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-dbe3ed15eff0481487933aa4d5ab9292 |
| Source note | uspto-grants-2013_12 |