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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1909255Generated: October 28, 2026

HCID 68351212, compound → HCID 68351184, compound

https://huagongshe.com/reaction/1909255

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68351212HCID 68351212—
SolventEthanolHCID 702—
SolventPalladiumHCID 23938—
ProductHCID 68351184HCID 6835118475.2%

Reaction Steps

To a stirred solution of ethyl 6-(1-(tert-butoxycarbonyl)-1,2,3,6-tetrahydropyridin-4-yl)-1-isopropyl-1H-pyrazolo[3,4-b]pyridine-4-carboxylate (0.45 g, 1.086 mmol) in EtOH (10 mL), 10% Pd/C in catalytic amount was added and stirred it at room temperature under hydrogen pressure (bladder pressure) for 3 hr. On completion of reaction, reaction mass was filtered through celite bed, then filtrate was concentrated under reduce pressure to give the desired compound (0.34 g, 75%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08598167B1
Source datasetuspto-grants-2013_12
ORD IDord-82d2e04c0e8e412291d32ae6153c4130
Source noteuspto-grants-2013_12