HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Oxolan-2-yl)acetic acid → HCID 178520298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Oxolan-2-yl)acetic acid | HCID 228726 | — |
| Reactant | HCID 178479251 | HCID 178479251 | — |
| Product | HCID 178520298 | HCID 178520298 | — |
Reaction Steps
The title compound, white solid (9 mg, 25%), MS (ISP) m/z=443.5 [(M+H)+], was prepared in accordance with the general method of example 1 from Trans-4-[2-(4-Benzo[1,3]dioxol-4-yl-piperidin-1-yl)-ethyl]-cyclohexylamine hydrochloride (intermediate A) (29.4 mg, 0.080 mmol) and 2-(tetrahydrofuran-2-yl)acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598357B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-1cb4f0cb2596499ca6139b9151df24a6 |
| Source note | uspto-grants-2013_12 |