HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanoacetic acid → HCID 178511189, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanoacetic acid | HCID 9740 | — |
| Reactant | HCID 178479251 | HCID 178479251 | — |
| Product | HCID 178511189 | HCID 178511189 | — |
Reaction Steps
The title compound, light yellow solid (14.9 mg, 53.5%), MS (ISP) m/z=398.1 [(M+H)+], was prepared in accordance with the general method of example 1 from Trans-4-[2-(4-Benzo[1,3]dioxol-4-yl-piperidin-1-yl)-ethyl]-cyclohexylamine hydrochloride (intermediate A) (25.7 mg, 0.07 mmol) and 2-cyanoacetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598357B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-c08cceae15e24cebad5fe20b49bf11ea |
| Source note | uspto-grants-2013_12 |