HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Difluorocyclopropane-1-carboxylic acid → HCID 178523608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Difluorocyclopropane-1-carboxylic acid | HCID 2782823 | — |
| Reactant | HCID 178479251 | HCID 178479251 | — |
| Product | HCID 178523608 | HCID 178523608 | — |
Reaction Steps
The title compound, white solid (9.7 mg, 31.9%), MS (ISP) m/z=435.4 [(M+H)+], was prepared in accordance with the general method of example 1 from Trans-4-[2-(4-Benzo[1,3]dioxol-4-yl-piperidin-1-yl)-ethyl]-cyclohexylamine hydrochloride (intermediate A) (25.7 mg, 0.070 mmol) and 2,2-difluorocyclopropanecarboxylic acid
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598357B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-d41dbefd9e8048f7a4e8c89684d5895d |
| Source note | uspto-grants-2013_12 |