HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxyisovaleric acid → HCID 178459207, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxyisovaleric acid | HCID 69362 | — |
| Reactant | HCID 178479251 | HCID 178479251 | — |
| Product | HCID 178459207 | HCID 178459207 | — |
Reaction Steps
The title compound, white solid (18.7 mg, 62%), MS (ISP) m/z=431.4 [(M+H)+], was prepared in accordance with the general method of example 1 from Trans-4-[2-(4-Benzo[1,3]dioxol-4-yl-piperidin-1-yl)-ethyl]-cyclohexylamine hydrochloride (intermediate A) (25.7 mg, 0.070 mmol) and 3-hydroxy-3-methylbutanoic acid
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598357B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-923bd602e0d4469f8d9521ac78c1f7a9 |
| Source note | uspto-grants-2013_12 |