HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dioxo-1lambda6-thiolane-3-carboxylic acid → HCID 178523620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dioxo-1lambda6-thiolane-3-carboxylic acid | HCID 428044 | — |
| Reactant | HCID 178479251 | HCID 178479251 | — |
| Product | HCID 178523620 | HCID 178523620 | — |
Reaction Steps
The title compound, white solid (21.1 mg, 54.1%), MS (ISP) m/z=477.2 [(M+H)+], was prepared in accordance with the general method of example 1 from Trans-4-[2-(4-Benzo[1,3]dioxol-4-yl-piperidin-1-yl)-ethyl]-cyclohexylamine hydrochloride (intermediate A) (30 mg, 0.0818 mmol) and 1,1-Dioxo-tetrahydro-thiophene-3-carboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598357B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-fd29e354b7f340d58c67529757937f6a |
| Source note | uspto-grants-2013_12 |