HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Aminosalicylic Acid → HCID 16042342, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Aminosalicylic Acid | HCID 4075 | — |
| Reactant | 1-(3-Bromopropyl)-4-nitrobenzene | HCID 10444482 | — |
| Product | HCID 16042342 | HCID 16042342 | 50.4% |
Reaction Steps
According to the similar procedure to Synthesis Example 1, by using 5-aminosalicylic acid (500 mg, 3.26 mmole) and 3-(4-nitrophenyl)propyl bromide (950 mg, 3.92 mmole), 520 mg (50% yield) of 2-hydroxy-5-[3-(4-nitrophenyl)-n-propylamino]-benzoic acid was obtained as a pale yellow solid. Melting point 229-231° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598383B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-8396d8c2a3674fafa38e7e749240050d |
| Source note | uspto-grants-2013_12 |