HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 44818810, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 44819172 | HCID 44819172 | — |
| Product | HCID 44818810 | HCID 44818810 | 49.5% |
Reaction Steps
Following the general procedure for Example 18, the product from step 1 (0.80 g 1.99 mmol) was treated with a 1:1 mixture of concentrated HCl/dioxane (36 mL) to afford the title compound (0.21 g, 26%) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598359B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-a8c7144870944941a72291a1907f9ade |
| Source note | uspto-grants-2013_12 |