Hydrochloric Acid → HCID 69001626, compound

Participants

Reaction Steps

To the product from step 2 (10 mg, 0.027 mmol) was added 3 ml of 2N HCl in diethyl ether. The resulting mixture was stirred at rt for 2 h. The solvent was removed to give the title compound (8 mg, 96%). MS; m/z 269 (M+H)>90% 1H NMR (DMSO-d6, 400 MHz) δ 1.59-2.12 (4H, m), 3.21 (2H, m), 3.90 (2H, s), 4.31 (1H, m), 4.46 (1H, dd, J1=4.0 Hz, J2=11.6 Hz), 6.80 (1H, d, J=8.4 Hz), 7.17-7.31 (5H, m), 7.57 (1H, dd, J1=2.4 Hz, J2=8.4 Hz), 8.09 (1H, d, J=2.4 Hz), 8.93 (1NH, s), 9.48 (1NH, s)

Provenance & Evidence