HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 69001877, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 68999301 | HCID 68999301 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic acid methanol | HCID 10129899 | — |
| Product | HCID 69001877 | HCID 69001877 | 83% |
Reaction Steps
To product from step 2 (50 mg, 0.13 mM) was added Pd/C 10% (40 mg, wt) in MeOH/AcOH (1.5 ml, 6:4) and stirred under H2 (H2 balloon, atm pr) for 6 h. 10% NaOH (5 mL) was added to quench the reaction. EtOAc was added and the mixture was filtered and dried down to give the title compound (29 mg, 83%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598359B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-de6711658d7848e5ada336e6d1c92723 |
| Source note | uspto-grants-2013_12 |