Boron tribromide → HCID 69003779, compound

HRID 1909801Notes

Reaction equation

HRID 1909801 reaction equation
C[O:2][C:3]1[CH:20]=[CH:19][C:6]([CH2:7][C:8]2[S:9][C:10]([C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=3)=[CH:11][CH:12]=2)=[CH:5][CH:4]=1.B(Br)(Br)Br>>[C:13]1([C:10]2[S:9][C:8]([CH2:7][C:6]3[CH:5]=[CH:4][C:3]([OH:2])=[CH:20][CH:19]=3)=[CH:12][CH:11]=2)[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=1

Participants

3

Reactant 2

HCID 25134Boron tribromideHCID 56986365HCID 56986365, compound

Product 1

HCID 69003779HCID 69003779, compoundYield 100.1%

Procedure

The title compound (480 mg, 99%) was prepared from the product of step 3 (0.50 g, 1.8 mmol) and BBr3 (1.3 g, 5.3 mmol) using the procedure of Example 146, step 2.

Sources & evidence

ORD record
ord-c39cc75c428843208e00ccd86712ac0c
Source dataset
uspto-grants-2013_12
Patent number
US08598359B2

Reaction notes

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