HuagongsheHuagongshe Chemistry Print Report · For research reference only
methyl 2-amino-1H-benzo[d]imidazole-4-carboxylate → HCID 66940377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | methyl 2-amino-1H-benzo[d]imidazole-4-carboxylate | HCID 24730367 | — |
| Reactant | Methyl 2-amino-5-methyl-3-nitrobenzoate | HCID 58213211 | — |
| Product | HCID 66940377 | HCID 66940377 | 85% |
Reaction Steps
0.3 g (85% overall yield) 2-amino-6-propyl-1H-benzoimidazole-4-carboxylic acid methyl ester was synthesized according to procedures described for the synthesis of 2-Amino-1H-benzoimidazole-4-carboxylic acid methyl ester (intermediate A) starting from 0.35 g (1.5 mmol) of above synthesized 2-amino-5-methyl-3-nitrobenzoic acid methyl ester. LCMS: 234 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598353B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-eed727d7f06f400b81f99c492cf891eb |
| Source note | uspto-grants-2013_12 |