HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66940393, compound → HCID 66940596, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66940393 | HCID 66940393 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66940596 | HCID 66940596 | — |
Reaction Steps
3.0 g (7.9 mmol) of 3-amino-5-benzyloxy-2-nitro-benzoic acid benzyl ester was reduced by 5.4 g (23.7 mmol) of SnCl22H2O in 30 mL of ethanol at 80° C. for 3 h to produce 2,3-diamino-5-benzyloxy-benzoic acid benzyl ester. LCMS: 350 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598353B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-88f62af3caee4fb9858b32f2d36bcaca |
| Source note | uspto-grants-2013_12 |