HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium ethoxide → HCID 86608395, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium ethoxide | HCID 2723922 | — |
| Reactant | HCID 86608394 | HCID 86608394 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86608395 | HCID 86608395 | — |
Reaction Steps
1.2 g (5.5 mmol) of 3-amino-4,5-difluoro-2-nitro-benzoic acid was heated with excess 21% NaOEt in ethanol at 90° C. for 6 h to yield 3-amino-5-ethoxy-4-fluoro-2-nitro-benzoic acid. LCMS: 245 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598353B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-6e5ef225e69544d39fea174254559467 |
| Source note | uspto-grants-2013_12 |