HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylphenyl boronic acid → HCID 59594033, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylphenyl boronic acid | HCID 2733267 | — |
| Reactant | 2-(3-Bromophenyl)pyridine | HCID 11115506 | — |
| Product | HCID 59594033 | HCID 59594033 | — |
Reaction Steps
2-(3-bromophenyl)pyridine (25.0 g, 0.107 mol) was reacted with 2-methylphenylboronic acid (17.4 g, 0.128 mol) under standard Suzuki coupling condition. The product (25 g) was collected by Kugelrohr distillation at 220° C. as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08603645B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-b3d5939825e84804b8495268c2207dde |
| Source note | uspto-grants-2013_12 |