HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethanol → 1-(2-Hydroxyethyl)-2,3,3-trimethyl-3H-indol-1-ium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethanol | HCID 12225 | — |
| Reactant | 3H-Indole, 2,3,3-trimethyl- | HCID 15427 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 1-(2-Hydroxyethyl)-2,3,3-trimethyl-3H-indol-1-ium iodide | HCID 13761015 | — |
Reaction Steps
In a particular example for the preparation, about 16 g of 2,3,3-trimethyl-3H-indole was dissolved in about 100 ml of chloroform. After addition of about 19 g of 2-Iodoethanol, the solution was refluxed while stirring for about 1 day. After cooling, the solvent was removed and the resultant solid was filtered and washed with acetone to yield 1-(2-hydroxyethyl)-2,3,3-trimethyl-3H-indolium iodide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08603944B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-4ae44de8776a46238153ff0833a97605 |
| Source note | uspto-grants-2013_12 |