Acetaldehyde → HCID 86664529, compound

Participants

Reaction Steps

[Step 1] 5 mL of a toluene suspension of 1.0 mg (3.5 mmol) of 6-aminoquinoline were added to 5 mL of a toluene suspension of 826 mg (3.5 mmol) of benzotriazole and stirred. 5 mL of a toluene solution containing 0.22 mL (3.8 mmol) of acetoaldehyde were dropped therein followed by stirring for 18 hours at room temperature. Following completion of the reaction, 15 mL of n-hexane were added followed by filtering out the solid. The solid was washed with n-hexane and dried under reduced pressure to obtain 20 g of N-[1-(1H-benzo[d][1,2,3]triazol-1-yl)ethyl]quinolin-6-amine in the form of a white solid (99%).

Provenance & Evidence