Acetaldehyde → HCID 86664535, compound

Participants

Reaction Steps

[Step 1] 10 mL of a toluene suspension containing 1.4 g (10 mmol) of benzo[d][1,3]dioxol-5-amine were added to 10 mL of a toluene suspension containing 1.2 g (10 mmol) of benzotriazole followed by stirring. 10 mL of a toluene solution containing 0.62 mL (11 mmol) of acetoaldehyde were dropped therein followed by stirring for 18 hours at room temperature. Following completion of the reaction, 10 mL of n-hexane were added followed by filtering out the solid. The solid was washed with n-hexane and dried under reduced pressure to obtain 2.7 g of N-[1-(1H-benzo[d][1,2,3]triazol-1-yl)ethyl]benzo[d][1,3]dioxol-5-amine in the form of a pale brown solid (94%).

Provenance & Evidence